Hach 29971-72 Руководство пользователя

DOC024.98.93010

ORBISPHERE Model 29971-72

08/2018, Edition 10

User Manual

Benutzerhandbuch

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Manual de usuario

Návod k použití

Gebruikershandleiding

Instrukcja obsługi

Manual de utilizare

Руководство пользователя

Felhasználói kézikönyv

English..............................................................................................................................3

Deutsch.......................................................................................................................... 23

Italiano............................................................................................................................ 44

Español.......................................................................................................................... 64

Čeština........................................................................................................................... 84

Nederlands................................................................................................................. 103

Polski............................................................................................................................ 123

Română....................................................................................................................... 144

Русский........................................................................................................................164

Magyar......................................................................................................................... 185

2

Table of contents

Specifications on page 3 Operation on page 15

General information on page 3 Maintenance on page 18

Installation on page 8 Troubleshooting on page 19

Startup on page 13 Replacement parts and accessories on page 19

Specifications

Specifications are subject to change without notice.

Specification Details

Dimensions (W x H x D)

20 × 75 × 40 cm (7⅞ × 29½ × 15¾ in.)

Weight 8.5 kg (18¾ lb)

Package height Minimum: 10 cm (3.94 in.)

Maximum: 36 cm (14.17 in.)

Package diameter

Maximum: 20 cm (7⅞ in.)

Purge gas supply Pure CO

2

or N

2

(with a minimum 99.8% purity)

Gas supply pressure Minimum: 0.8 bar (12 PSI)

Maximum: 3 bar (43 PSI)

Gas supply flow 10 to 50 mL/min

General information

In no event will the manufacturer be liable for direct, indirect, special, incidental or consequential

damages resulting from any defect or omission in this manual. The manufacturer reserves the right to

make changes in this manual and the products it describes at any time, without notice or obligation.

Revised editions are found on the manufacturer’s website.

Safety information

N O T I C E

The manufacturer is not responsible for any damages due to misapplication or misuse of this product including,

without limitation, direct, incidental and consequential damages, and disclaims such damages to the full extent

permitted under applicable law. The user is solely responsible to identify critical application risks and install

appropriate mechanisms to protect processes during a possible equipment malfunction.

Please read this entire manual before unpacking, setting up or operating this equipment. Pay

attention to all danger and caution statements. Failure to do so could result in serious injury to the

operator or damage to the equipment.

Make sure that the protection provided by this equipment is not impaired. Do not use or install this

equipment in any manner other than that specified in this manual.

Use of hazard information

D A N G E R

Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.

W A R N I N G

Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious

injury.

English 3

C A U T I O N

Indicates a potentially hazardous situation that may result in minor or moderate injury.

N O T I C E

Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special

emphasis.

Precautionary labels

Read all labels and tags attached to the instrument. Personal injury or damage to the instrument

could occur if not observed. A symbol on the instrument is referenced in the manual with a

precautionary statement.

This is the safety alert symbol. Obey all safety messages that follow this symbol to avoid potential

injury. If on the instrument, refer to the instruction manual for operation or safety information.

This symbol indicates a potential pinch hazard.

Electrical equipment marked with this symbol may not be disposed of in European domestic or

public disposal systems. Return old or end-of-life equipment to the manufacturer for disposal at no

charge to the user.

This symbol indicates the need for protective eye wear.

This symbol indicates the need for protective hand wear.

Product overview

The beverage package sampler system is used to measure the gas concentrations of a beverage.

There are two different models of the beverage package sampler: one for wine (or still liquids)

sampling and the other for beer (or carbonated liquids) sampling. Refer to Table 1 and Figure 1.

Table 1 Sampling systems

Sampler Application Examples

Model 29971 on page 5 Non-carbonated liquids and liquids without

suspended particles

Wine, mineral water, etc.

Model 29972 on page 7 Carbonated liquids and liquids with

suspended particles

Beer, mineral water, sparkling wine,

fruit juices, alcopops, etc.

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Figure 1 Beverage package sampler

1 Flow chamber 4 Orange securing handle

2 Piercing head 5 To indicating instrument

3 Piercing lever 6 Package sampler sensor

Model 29971

Model 29971 measures gas concentrations in wine or non-carbonated liquids. Refer to Figure 2 and

Replacement parts—Piercing head on page 20.

For wine sampling, use the model 29971 with the piercing head model 29973 pre-assembled. Refer

to photo R in Figure 2. The piercing needle assembly (R3 in Figure 2) pierces wine bottles with all

type of corks and has a moveable stainless steel needle within a fixed cylindrical tube. The piercing

head holder plate (R6 in Figure 2) has a sealing assembly for a perfect seal between the bottle corks

and the external medium. Make sure that the silicone sealing plug (R4 in Figure 2) is included for a

correct and tighter seal.

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Figure 2 Piercing heads—Photo Q 29974, Photo R 29973

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Model 29972

Model 29972 measures gas concentrations in beer or carbonated liquids. There are two models:

• Model 29972 is used with an electrochemical (EC) sensor.

• Model 29972.M is used with a luminescent dissolved oxygen (LDO) sensor.

The two models include the piercing head model 29974 pre-assembled. Refer to photo Q in Figure 2

on page 6.

The piercing needle assembly (Q3 in Figure 2 on page 6) pierces cans, metal or plastic caps or

crowns used in the beer industry. The piercing assembly has a piercer tube surrounded by a rubber

seal (Q4 in Figure 2 on page 6) for a perfect sealing between the bottle cap and the external

medium, within which the stainless steel cylindrical sampling tube can move. There are two types of

piercing knifes (Q35 in Figure 2 on page 6):

• Model 28072 for piercing metal caps

• Model 29979 for piercing PET bottles or plastic caps

Theory of operation

The beverage package sampler is used with an ORBISPHERE indicating instrument for analysis of

the oxygen, carbon dioxide and/or nitrogen gas content of a beverage. The ORBISPHERE indicating

instrument is supplied separately.

The indicating instrument reads and shows the measurement data from the package sampler sensor.

The indicating instrument is available in a portable, panel or wall mount version. Different indicating

instruments can be used. Refer to the indicating instrument documentation for additional information

(e.g., installation procedures, electrical connections).

The beverage package sampler holds the package sample being analyzed. A separate supply of

forcing gas moves the package liquid to the flow chamber, where the senor is installed. The sensor

and flow chamber are installed on the side of the sampler in a special sensor holder. The flow

chamber pulls liquid samples from the beverage sampler (e.g., bottle, can) to the sensor for analysis.

Different types of flow chambers are available for the different beverage package sampler

applications. The indicating instrument senses and shows on the display the package gas

concentration. The complete system supplies electrical and liquid connections to the instrument, to

the sensors and to the gas supplies.

Note: This manual is applicable to the ORBISPHERE Beverage Package Sampler models 29971 and 29972. Refer

to the user manual supplied with the gas analyzer indicating instrument that is used with the beverage package

sampler.

Product components

Make sure that all components have been received. If any items are missing or damaged, contact the

manufacturer or a sales representative immediately.

• Beverage package sampler

• Flow chamber

• Package sampler sensor: The sensor supplied is based on the instrument model and the beverage

sampler application. One of the package sampler sensors that follow:

• Electrochemical (EC) sensor for dissolved oxygen

• Luminescent Dissolved Oxygen (LDO) sensor

• Carbon dioxide (CO

2

) sensor

• Nitrogen (N

2

) sensor

• Plastic tubing for liquid connections, 5 m (16.40 ft)

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• Short length plastic tubing for purge gas exit connection, 8 cm (3.15 in.)

Installation

D A N G E R

Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the

document.

Installation overview

Figure 3 shows the electrical, liquid and gas connections for a typical sensor installation.

Figure 3 System schematic—Electrical, liquid, and gas connections

1 Gas flow 6 Liquid drain 11 Sampling tube

2 Regulator 7 Purge gas exit 12 Forcing gas entrance port

3 Indicating instrument 8 Sensor 13 Forcing and purge gas

4 Connectors 9 Liquid flow

5 Temperature sensor 10 Beverage sampler

Assemble the EC/TC sensor

N O T I C E

If tubing replacement is necessary, make sure to use material of low gas permeability, such as flexible nylon,

PVC, or tygon for tube replacement. Do not use metal tubing or damage to the brass connectors can occur.

Refer to Figure 4 and do the steps that follow to assemble the system:

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English

1. Carefully put the flow chamber on the sensor head in the sensor holder (E). Make sure not to

touch the membrane or damage to the membrane can occur. Tightly screw the sensor collar to

attach the flow chamber into its location.

2. Put the LEMO plug that is on the end of the sensor cable into the sensor socket of the indicating

instrument.

3. Connect approximately 25 cm of plastic tube from the top of the piercing head (A) to the inlet

Swagelok fitting on the flow chamber.

4. Connect the gas supply as follows:

a. Connect the gas supply to the 6 mm brass Swagelok gas supply connector assembly (D) on

the sensor holder (E) with a nylon tube.

b. Connect the brass Swagelok gas supply to the lower piercing column Swagelok assembly (C)

with a nylon tube.

c. Use the knurled screw (B) on the same black block as the gas inlet port as a gas on/off valve.

Note: Use nitrogen or carbon dioxide as the forcing gas supply based on the beverage package application.

5. Make sure that all Swagelok fittings are tight.

Figure 4 EC/TC sensor sampler assembly

Assemble the LDO sensor

N O T I C E

If tubing replacement is necessary, make sure to use material of low gas permeability, such as flexible nylon,

PVC, or tygon for tube replacement. Do not use metal tubing or damage to the brass connectors can occur.

Refer to Figure 5 and do the steps that follow to assemble the system:

1. Install the U-shaped ring to hold the flow chamber on the correct position (D).

2. Put the flow chamber in the correct position (D). Make sure that the tubing points to the front.

Tighten the screws of the U-shaped ring to attach the flow chamber into its location.

3. Install the LDO sensor in the flow chamber. Tighten the screw in the collar on the LDO sensor to

the flow chamber.

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4. Put the LEMO plug that is on the end of the sensor cable into the sensor socket of the indicating

instrument.

5. Connect the inlet tube of the flow chamber to the (A) position on the top of the piercing head.

Note: Use two open-end wrench (16 and 15 mm) to firmly tighten the assembly. Make sure not to damage the

POM part.

6. Cut the correct length of plastic tube to connect the outlet of the flow chamber to the waste.

Connect the tube to the valve outlet of the flow chamber.

7. Connect the gas supply to push the liquid through the flow chamber. Use a nylon tube to connect

the gas supply to the lower piercing column Swagelok assembly (C). A knurled screw (B) that is

on the same black block as the gas inlet port operates as a gas on/off valve.

Note: Use nitrogen or carbon dioxide as the forcing gas supply based on the beverage package application.

8. Make sure that all Swagelok fittings are tight so the beverage package sampler operates

correctly.

Figure 5 LDO sensor sampler assembly

Connect the gas purge

N O T I C E

Do not put the CO

2

or N

2

sensor into a liquid sample until the purge gas connection is complete. Water can

condense in the measuring chamber if the unit is not operating and damage to the sensor will occur.

Use stainless steel or plastic tubing (e.g., nylon, tygon or PVC) to connect the gas purge line to the

sensor.

1. Use a 14 mm wrench to attach the purge gas tube to the 6 mm Swagelok fitting that is on the

sensor.

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English

For the first intallation, tighten the fitting by hand. Use the wrench to tighten the fittings another ¼

turn.

2. Install the purge gas outlet with the supplied short length plastic tube. Put the plastic tube in the

orifice opposite the purge gas inlet and push firmly. To remove the tube, push on the ring around

the tube and pull.

3. Make sure that there is no loss of purge gas supply while the sensor is in a liquid sample and

always when the sensor is in line. If necessary, use a backup purge gas cylinder and an

automatic change-over valve, which operates when the first cylinders gas supply has expired.

Change-over valves are frequently known as flip-flop valves and are available from local gas

regulator suppliers.

4. Examine the purge gas flow rate as follows:

a. Connect the sensor to the instrument. Set the instrument to on. The inner solenoid valve in

the sensor opens and lets the gas to flow.

b. Put the open end of the exit tube in water.

c. Adjust the gas flow rate so that there is a minimum of three bubbles each second.

d. Remove the exit tube from the water.

Note: Do not keep the exit tube in the water, because water can go back in the tube and cause damage to

the CO

2

sensor.

Install a regulator and filter (optional)

When the beverage package sampler is used for analysis of the CO

2

or N

2

content of a liquid, a TC

sensor is used. TC sensors must have a constant supply of purge gas for operation. The regulator

keeps a constant pressure of the purge gas to the TC sensor.

Use the optional ORBISPHERE model 29089 regulator and filter to make sure that the purge gas is

dry and kept at a correct pressure. The regulator is connected in-line with the purge gas supply,

directly to the purge gas entry port of the TC sensor. Install the regulator with the supplied stainless-

steel tubing connected to the CO

2

or N

2

sensor. Make sure to install the regulator vertical (±5%).

Obey the flow direction: from left to right (with the gauge in the front). Refer to Figure 6.

A gauge on the regulator shows the pressure of the gas. Turn the pressure adjuster knob on the top

of the unit to adjust the pressure of the purge gas. Refer to Specifications on page 3 for the correct

gas pressure.

Make sure to drain the condensate at periodic intervals for a correct compressed air filter

maintenance. Open the condensate bleed screw to blow the moisture with pressure. Refer to

Figure 6.The filter is made of sintered metal. An O-ring keeps the filter in the correct position when

the filter bowl is removed. Clean or replace the filter if the filter becomes heavily contaminated. Use

rinsing water and compressed air to clean the filter.

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Figure 6 Model 29089 regulator and filter

1 Inlet, 6 mm (1/4 in.) 6 Filter

2 Gauge 7 Filter holding nut

3 Pressure adjuster 8 Filter cover

4 Outlet, 6 mm (1/4 in.) 9 Condensate bleed screw

5 Coverplate (behind gauge)

Model 31560 or 31590—N

2

sensor

Use pure CO

2

from a cylinder for the purge gas for N

2

sensors. Make sure that the flow rate and

pressure do not exceed the values in Specifications on page 3.

Note: Do not use more than the recommended purge gas pressure. Too much pressure will inflate the sensing

membrane and give incorrect measurements.

Model 31460 or 31490—CO

2

sensor

Use nitrogen for the purge gas for CO

2

sensors. A source of reasonably pure purge gas is necessary

(e.g., 99.8%). Install a sub-micron filter before the CO

2

sensor if clean, dry air or bulk nitrogen is used

as purge gas. Make sure that the flow rate and pressure do not exceed the values in Specifications

on page 3.

Note: Do not use more than the recommended purge gas pressure. Too much pressure will inflate the sensing

membrane and give incorrect measurements.

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English

Install the optional piercing head

The system has one of the two piercing head models installed: 29973 or 29974. Refer to the steps

that follow to change the piercing head if necessary.

1. Push up the piercing lever to a vertical position to lift the piercing unit.

2. Lock the piercing unit with the orange vertical handle.

3. Disconnect the beverage outlet tubing from the top of the piercing head (A in Figure 4 on page 9).

4. Disconnect the gas inlet tubing from the bottom of the piercing head (C in Figure 4 on page 9).

5. Remove the two Allen-head screws that attach the piercing head support plate to the moveable

piercing unit.

6. Remove the two Allen-head screws that attach the piercing column to the piercing arm of the unit.

7. Remove the piercing head.

8. Tighten the new piercing head to the piercing arm of the unit with the two bolts. Make sure that

the Swagelok fittings points towards the inlet and outlet plastic tubes.

9. Tighten the new piercing head support plate to the moveable piercing unit with the two bolts.

10. Connect the gas inlet plastic tube to the bottom of the piercing head on the bottom black block (C

Figure 4 on page 9).

11. Connect the beverage outlet plastic tube to the top of the piercing head on the top black block (C

Figure 4 on page 9).

Connect the indicating instrument

The electrical connections for the indicating instrument are on the rear panel of the instrument. The

rear panel has a power connector for the power cable and a LEMO-10 connector for the O

2

, CO

2

or

N

2

sensor that is used with the beverage sampler. Refer to the indicating instrument documentation

for installation information.

Startup

C A U T I O N

Personal injury hazard. Glass components can break. Handle with care to prevent cuts.

Before measurements are started, do the steps that follow:

1. Make sure that the indicating instrument is correctly installed and configured. Refer to the

indicating instrument documentation.

2. Make sure that the connections between the indicating instrument and the sensor(s) on the

beverage package sampler are correct.

3. Always keep the indicating instrument energized to make sure that TC sensors are continuously

purged when the sensors are used in a liquid sample.

Note: The instrument is configured to continuously purge automatically while set to on.

4. Examine and prepare the sensors as follows:

a. Examine the oxygen sensor (EC). Shipping conditions can adversely have an effect on

oxygen sensors. Prepare the sensor for use. Refer to the maintenance section of the EC

Sensor documentation.

b. Examine the oxygen sensor (LDO). Prepare the sensor for use. Refer to the sensor

documentation.

c. Examine the TC sensor purge gas supply. Make sure that the gas supply operates before the

CO

2

or N

2

sensors are installed in-line. When the TC sensors are in touch with a liquid

sample, damage to the sensor can easily occur if the purge gas is not operative. Refer to

Connect the gas purge on page 10.

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5. Make sure that the gas pressure is 0.5 to 1 bar more than the dissolved CO

2

pressure of the

sample. Do not exceed the maximum permitted pressure for the package (bottle or can) or the

package could explode. For measurements with TC sensors, it is important to use the same

forcing gas pressure for both: calibration and gas measurement operations.

6. Shake the package, if applicable. In some beverage sampling applications, it is necessary to

shake the beverage packages to equilibrate the contents of the package. Use a reciprocating

shaker for a minimum of 3 minutes.

Indicating instrument setup

Make sure that the indicating instrument setup is completed before the measurements are started.

Configure parameters such as the gas to measure, the display units and the sensor membrane used.

Refer to the indicating instrument documentation for additional information.

Adjust the package position

Before the measurements are started, adjust the beverage package sampler for the type of beverage

sample container (bottle or can). Refer to Figure 7 and to the steps that follow:

1. Push the top (moveable) black block to the highest position (A) to lift the piercing and sampling

assembly.

2. Make sure that the piercing lever (B) is in a vertical position.

3. Hold the piercing unit sliding assembly with one hand and loosen the orange handle (C).

4. Lift the piercing unit sliding assembly upwards on the two metal columns.

5. Put the beverage sample to be analyzed on the mat of the base plate (D).

Make sure to vertically install the beverage sample. If possible, pierce cans through the top. If

there is not sufficient area for piercing in the top of the can because of the tab, then pierce

through the bottom. Piercing through the bottom has the advantage that the metal is thicker and

less easily deformed, but sometimes has the disadvantage that the piercing needle becomes

immersed in the beverage.

6. Lower the piercing unit carefully until the piercing head support plate with the circular hole

touches the top of the beverage sample (E). The piercing head support prevents unwanted

movement of the beverage sample.

7. Lift the orange handle to the upper position of the groove and tighten it again.

The unit is prepared for measurement.

Note: If the type of package sample is changed, such as a different dimension bottle or can, do the adjust package

procedure again.

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English

Figure 7 Package adjustment

Operation

C A U T I O N

Personal injury hazard. Glass components can break. Handle with care to prevent cuts.

User controls

The user controls are:

• Orange vertical position lever—Adjusts the height of the unit for different packages

• Lateral protective plates—Adjust the height of the unit

• Piercing lever—Lowers or lifts the piercing unit to pierce the package

• Piercing and sampling assembly—Lowers or lifts the sampling tube into the package liquid

contents

Measure a package—Bottles

Pre-requisite: Complete all of the preliminary checks in Startup on page 13.

1. Put the beverage sampler below the hole of the piercing head support plate and adjust the

package to the center.

Note: The manufacturer recommends that the bottle protection is used in bottle measurements. Put the bottle

in the bottle protection. Make sure that the bottle cap is at the same level as the bottle protection. Add or

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remove the discs supplied with the bottle protection to adjust the height of the bottle (supplied discs: 6, 20 and

50 mm).

2. Pull the piercing lever to the horizontal position to pierce the beverage sample cork, crown or cap.

3. Use the top black block on the piercing head to lower the sampling tube to near the bottom of the

beverage sample. Refer to Figure 8.

4. Set the gas pressure and open the on/off valve on the lower block of the piercing head (F). Adjust

the flow rate to approximately 200 mL/minute for carbonated beverages or 100 mL/minute for

non-carbonated beverages.

• For wine flow rate, and for liquids with suspended particles, use the pressure control valve at

the gas source.

• For sparkling liquids, use the screw at the top of the flow chamber.

5. If bubbles are seen in the tubing, change the flow rate of the liquid and/or the gas pressure to

remove the bubbles. The applied gas pressure must be more than the dissolved CO

2

pressure in

carbonated liquids.

6. Wait until the gas concentration that shows on the instrument display is stable. Record the

measurement value.

Note: Some indicating instruments automatically record the measurement value when a PC is connected to the

instrument. Refer to the indicating instrument documentation for the correct measurement procedure.

7. When the gas measurement is complete for the package sample, do the steps that follow:

a. Close the on/off gas valve on the lower block of the piercing head.

b. Lift the sample tube up to the highest position.

c. Push the piercing lever to the vertical position.

d. Remove the beverage sample.

Figure 8 Package measurement

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Flush the system

When a series of analyses is complete, flush the system with warm water as follows:

1. Discard the content of the beverage package.

2. Fill the package with water.

3. Use the available gas pressure to flush the water through the system.

Sensor calibration

Refer to the indicating instrument and sensor documentation for the calibration requirements and

procedures for the sensor.

Optional devices and accessories

One or more of the optional items that follow are necessary based on the user application. Contact

your Hach representative for more information.

Model 29089—Regulator and filter

Refer to Install a regulator and filter (optional) on page 11.

Model 32301—Sensor cleaning and regeneration center

The model 32301 sensor cleaning and regeneration center is a multi-function device for

ORBISPHERE electrochemical (EC) sensors. Use model 32301 to:

• Clean the sensor electrodes.

• Examine the sensor for correct operation or to find a fault.

Model 32559—External temperature sensor

The model 32559 external temperature sensor is available for applications where the sample

temperature can continuously change. The external temperature sensor supplies a constant sample

temperature signal independently from the room temperature.

The temperature sensor is installed directly in the flow chamber. The temperature sensor is

connected with a cable with a LEMO-4 connector to a junction box that is installed at the rear of the

TC sensor.

Model 32605—Purge gas backup unit

The user must keep the indicating instrument always set to on to continuously apply purge gas to the

CO

2

(or N

2

) sensor and prevent sensor damage, even when there is no CO

2

(or N

2

) analysis. Use

the purge gas backup unit, model 32605, to set the indicating instrument to off without removing the

sensor from the flow chamber. The purge gas backup unit lets the user set the indicating instrument

to off.

Install the purge gas backup unit directly between the instrument and the sensor through the sensor

cable. The unit is energized by internal batteries. The internal batteries are automatically recharged

when the instrument is set to on. When the instrument is set to off, the purge backup unit continues

to purge the sensor for a maximum of 4 days.

Model 32816—Reciprocating shaker

In some beverage sampling applications, it is necessary to shake the beverage packages to

equilibrate the contents of the package.

If applicable, use the reciprocating shaker for a minimum of 3 minutes. The reciprocating shaker,

model 32816, operates at a frequency of 280 cycles/minute, with an amplitude of approximately 5 cm

(2 in).

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Maintenance

W A R N I N G

Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the

document.

The system has a special anti-corrosive treatment and does not require grease to be added during its

service life. Usually, maintenance tasks are only necessary on the sensor(s).

Maintenance schedule

Table 2 shows the recommended schedule of maintenance tasks. Facility requirements and

operating conditions may increase the frequency of some tasks.

Table 2 Maintenance schedule

Task 1 day 1 week As necessary

Clean the instrument on page 18 X X

Clean spills on page 18 X X

Clean the sensor on page 18 X

Clean the instrument

N O T I C E

Never use flammable or corrosive solvents to clean any part of the instrument. Use of these solvents can degrade

the environmental protection of the instrument and may void the warranty.

Clean the exterior surface with a moist cloth or with a mixture of water and mild detergent. Dry with a

soft cloth.

The manufacturer strongly recommends to clean the system after a series of analysis is complete or

at minimum daily. Use warm water (40 ºC, 104 ºF) to clean the system. Rinse the water through the

circuit for 5 minutes or 1 L at standard flow.

Clean spills

Clean all spills. Use a tissue on the platform to absorb spills.

1. Obey all facility safety protocols for spill control.

2. Discard the waste according to applicable regulations.

Clean the sensor

Refer to the documentation supplied with the sensor for maintenance instructions.

Do sensor maintenance when there are:

• Calibration problems

• An unusually long stabilization times, either with the sensor exposed to an air-saturated medium or

to different oxygen concentration conditions

• Noise or drift signals in constant oxygen concentration conditions

Regular maintenance is not necessary in CO

2

or N

2

TC sensors.

Note: While the membrane replacement procedure for CO

2

or N

2

TC sensors is equivalent to that of the EC sensor,

no chemical or electrochemical cleaning is necessary. In addition, membrane changes are much less frequent, if

applicable.

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English

Short-term storage

For short-term periods (less than one week), keep the sensors in the flow chamber. Make sure that

purge gas is constantly supplied to the TC sensor. Keep the indicating instrument energized or use a

purge gas backup unit.

Long-term storage

For long-term storage (more than one week), remove the sensor from the flow chamber. Refer to the

documentation supplied with the sensor for instructions on how to remove, clean and store the

sensors.

Clean the LDO sensor with water and put the protection cap on the collar to keep the membrane

away from light. Do not use chemicals to clean the LDO sensor or damage to the membrane can

occur.

Troubleshooting

Problem Possible cause Solution

There is beverage

sample suction

through the gas

supply.

The gas supply is

disconnected with the

system still under pressure.

Flush the gas tubing through with water. Dry the tubing with

a jet of gas.

No beverage flows

in the tubing.

There are defective fittings

or tubing connections.

Examine all Swagelok fittings and tubing connections for

leaks.

Use two wrenches to adjust the fittings. Examine the fitting

on the flow chamber, which can split if there is too much

pressure.

No beverage flows

in the tubing.

There is a blockage in the

inlet or outlet ports of the

flow chamber.

Make sure that the inlet and outlet ports of the flow chamber

are not clogged.

1. Carefully remove the nuts that attach the tubing in the

Swagelok inlet or outlet fittings of the flow chamber.

2. Clean and flush the flow chamber with hot water.

3. Let the flow chamber dry.

4. Assemble the flow chamber.

Note: Refer to the sensor documentation for additional information.

Replacement parts and accessories

W A R N I N G

Personal injury hazard. Use of non-approved parts may cause personal injury, damage to the

instrument or equipment malfunction. The replacement parts in this section are approved by the

manufacturer.

Note: Product and Article numbers may vary for some selling regions. Contact the appropriate distributor or refer to

the company website for contact information.

Accessories

Description Item no.

Pressure regulator kit 29089xx

Electrochemical sensor cleaning and regeneration unit 32301.x

External temperature sensor for off-line use, supplied with 4-pin LEMO connector for

TC sensors equipped with sensor adapter 32558. T-piece for connection to tubing is

included

32559.x

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Accessories (continued)

Description Item no.

Purge Backup Unit for TC sensors 32605

Reciprocating shaker, including package holder, universal voltage 32816

Adapter to upgrade piercer for LDO use DG33581

Replacement parts

Description Item no.

Lever handle grip for piercers 28073

Blue mat for piercers 28076

Supplemental piercing head for non-carbonated liquids 29973

Supplemental piercing head for carbonated liquids 29974

Replacement parts—Piercing head

The position number in Table 3 and Table 4 refers to the numbers in the photos illustrated in Figure 2

on page 6.

Table 3 29973 Piercing head for wine—Photo R

Position Item no. Description

1 — Swagelok assembly, brass, 6 mm

2 — Swagelok assembly, brass, 6 mm

3 28050 Piercing needle assembly, piercing head 29973

4 28051 Silicone seal, piercing head 29973

5 28043 Needle valve screw for lower black blocks 28052 and 28068, piercing heads 29973 and

29974

6 28044 Piercing head support plate for bottles, piercing heads 29973 and 29974

7 28045 Upper sampling assembly control, 29973 and 29974 piercing heads (includes Swagelok)

8 28052 Lower black block, including Swagelok assembly, piercing head 29973

17 28053 Piercing needle guide for piercing head support plate 28044, piercing head 29973

18 28054.4 Kit O-rings, nitril, 18 x 2 mm, 5 pieces

19 28055 Silicone sleeve for piercing head support plate 28044, piercing head 29973

20 — Piercing head cylindrical guides

21 28006S6 Swagelok front and back ferrule, 6 mm fittings

22

23 — Piercing column support plate

24 — Support plate screws, allen head

25 — Piercing head screws, allen head

26 28059 Piercing needle tube, piercing head 29973

27 28060 Piercing needle screw, piercing head 29973

20 English

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Hach 29971-72 Руководство пользователя

Hach 29971-72 Руководство пользователя

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